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VOC analysis results, sample AE03015, Feb 15 2002

Machine-extracted title · confidence 95%

Laboratory results for volatile organic compounds in sample AE03015 analyzed on February 15, 2002.

NYC-WTC_000019799–000019979

Folder label: “524 2/15/02 - 2/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\O2FEB15\03251.D Vial: 25 Acq On : 16 Feb 2002 3:55 am Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 Urea, ethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 15.79 0.04 ug/L 37226 1,4-DIFLUOROBENZENE 15.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Urea, ethyl- 88 C3H8N20 000625-52-5 4 2 1,4-Butanediamine 88 C4H12N2 000110-60-1 3 3 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O21 006843-45-4 3 4 1- (Propenyl thio) prop-l-ene 114 C6H10S 000000-00-0 3 Abundance Scan 684 (15.791 min): 03251 .D (-) m/z 114.05 100.00% 1 4

5000

63 88 15.40 15.60 15.80 16.00 16.20 44 50 **- | m/z 63.05 22.38% ■ i ■1 ■ ■ i ■ ■ ■ ■ i • 1133 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #789: Urea, ethyl- 33 44 73 88 5000 l ‘ ' I ' ‘ H • • i • • • > i • • 15.40 15.60 15.80 16.00 16.20 m/z 88.10 20.85% 56

/z-> 10 — 20 30 ■' i 40 LH+ 50 60 70 80 90 100 * i • ■ * < i • 110 120 Abundance #828: 1,4-Butanediamine 33

T-r-r-r-r-p-r -n-p-n-r-p-r 15.40 15.60 15.80 16.00 16.20 5000 m/z 57.05 12.65% 43

i , 59

m/z--> ‘1′111111 10 20 30 40 50 LL60 70 88 ■ ■ ■ I'' ■ ■ ■ i ■ ■ ■11 ■ ■1 ■ ................. .

70 80 90 100 110 120 Abundance #64088:2,4-Imidazolidinedione, 3-methyl- ________ I r 1 4 i 1 ' 4 ‘ J ' * ‘ ‘ I 1‘**‘i‘* 15.40 15.60 15.80 16.00 16.20 m/z 50.05 10.78% A 58 5000

86

42 71 t I 'T1' • • I * ‘ •l 1 • • ’ I • • ' ‘ I ’ ’ ' I ‘ 1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00 16.20

03251.D HP021302.M Mon Feb 18 15:28:00 2002 Page 1

NYC-WTC_000019912

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NYC-WTC_000019912Source: NYC Law Department, mirrored locally

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