Volatile organic compounds results, Mar 13 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\O2MAR20\6048A.D Vial: 14 Acq On : 20 Mar 2002 11:15 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : March 20, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Urea, ethyl- Concentration Rank I R.T. EstConc Area Relative to ISTD R.T. 15.78 0.03 ug/L 19681 1,4-DIFLUOROBENZENE 15.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Urea, ethyl- 88 C3H8N20 000625-52-5 4 2 Tetramethylhydrazine 88 C4H12N2 006415-12-9 4 3 Butane, 2-(ethenyloxy)-2-methyl- 114 C7H140 029281-39-8 3 4 4-Heptanone 114 C7H140 ______ 000123-19-3 3 Abundance Scan 694 (15.784 min): 6048A.D (-) m/z 114.15 100.00% 1’4

5000 63 88 A... .............. 15.40 15.60 15.80 16.00 ................................. 44 *1****1-44144**14 m/z 62.95 32.38% i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ i •1 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #789: Urea, ethyl- 33 44 73 88 5000 i ■ ■ ' ■ i ' ■ ■ ‘ i ' ‘ ‘ ' i ' 15.40 15.60 15.80 16.00 m/z 88.10 20.91% 56

m/z-> 1..7. 10 20 30 -n-p Immmp 40 50 60 70 80 90 100 110 120 Abundance #830: Tetramethylhydrazine 42 88 I ' 1 1 'i ' ' TT-p-n-r-p- 15.40 15.60 15.80 16.00 73 m/z 44.00 1.05% 5000 15

30

H ' "'I | 58 ■ J1^ "I" i ■ ■ ■ ■ i ■' ■111''' i'1 WWAMonM TT-p m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #3032: Butane, 2-(ethenyloxy)-2-methyl- 43 15.40 15.60 15.80 16.00

5000

55 71 85

m/z--> 27 991 ................. | ' ।' 111' ‘ I' ren । • । 4a । T-p-TTT-p-TT-rp-r ‘11 ■ • ■ ‘ i ■' ■ ‘ i ‘ 10 20 30 40 50 60 70 80 90 100 110 .1 120

6048A.D HP031802.M Fri Mar 22 09:52:29 2002 Page 1

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