Volatile organic compounds results, Mar 14 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02MAR14\06305.D Vial: 17 Acq On : 14 Mar 2002 11:55 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Urea, ethyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.75 0.03 ug/L 18796 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Urea, ethyl- 88 C3H8N20 000625-52-5 4 2 Tetramethylhydrazine 88 C4H12N2 006415-12-9 4 3 4-Heptanone 114 C7H14O 000123-19-3 3 4 Butane, 2-(ethenyloxy)-2-methyl- 114 C7H14O ______ 029281-39-8 3 Abundance Scan 692 (15.750 min): 06305.D (-) m/z 114.05 100.00% 1 4

5000

63 88 ‘ i * > • • i T1 15.40 15.60 15.80 16.00 44 1111117111 ' ' l " m/z 88.10 26.50% ■ ■ i ■' ■ ■ i ■' ■11 ■ ■'' i ■1 ■ ■ i ■ ‘ ■ ■ i ■ ■ ■ ■ i ■1 ■ ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #789: Urea, ethyl- 30 44 73 88 5000 15.40 15.60 15.80 16.00 m/z 63.05 25.82%

m/z-> 10 17 I'1 11 " 11 111 20 30 ■ ■ i 40 L 90 100 110 120 50 56 60 70 80 Abundance #830: Tetramethylhydrazine 42 88 ’1444*1** ' i ■ ■ ■ ■ i • • ■ ■ i1 15.40 15.60 15.80 16.00 73 5000 15 m/z 44.00 9.08

30 58 AMM 111 ■'' ■ i •' ■ ■ 11 1 ' 1 - i' ■ • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #3002:4-Heptanone 43 TI ill 15.40 15.60 15.80 16.00 71

5000 27

15 58 114 I ■ ■ i ■ ■ ■ ■ i ■ TTT — — ■ I,1 ■'' i ■111 86 99 | 11' "'111'' 1'1'111' m/z—> 10 20 30 40 50 60 70 80 90 100 110 120

06305.D HP031802.M Tue Mar 26 16:48:57 2002 Page 1

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