VOC analysis results, sample AE02575, Feb 8 2002

NYC 9/11 Public Portal Document 2\SpOL U (IOL KevLewed) s oid Data File C:\HPCHEM\l\DATA\02FEB08\0208C10D.D Vial: 11 Acq On 9 Feb 2002 1:08 am c Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 aalb MS Integration Params: LSCINT.P Quant Time: Feb 11 16:21 2002 Quant Results File: HP021102. Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Feb 11 15:54:13 2002 Response via : Initial Calibration DataAcq Meth : HP020502

Internal Standards R.T. Qlon Response Cone Units Dev(Min) —• ——— ———————————————————————————— ———————— nil 1) 1,4-DIFLUOROBENZENE 15.11 114 1851542 5.00 ug/L 0.00 24) CHLOROBENZENE-D5 21.76 117 1839799 5.00 ug/L 0.00 11 'Um

52) 1,4-DICHLOROBENZENE-D4 26.93 152 843848 5.00 ug/L -0.02 tt System Monitoring Compounds alft th 2) 1,2-DICHLOROETHANE-D4 14.35 65 735529 5.22 ug/L 0.00 Spiked Amount 5.000 Recovery = 104.40% 3) 4-BROMOFLUOROBENZENE 24.34 174 681596 4.90 ug/L -0.02 . Spiked Amount 5.000 Recovery = 98.00% 25) TOLUENE-D8 18.45 98 2291796 5.02 ug/L -0.02 “ -ortise Spiked Amount 5.000 Recovery = 100.40% Target Compounds 1/ Qvalue —s 4) DICHLORODIFLUOROMETHANE 4.87 85 784216 11.17 ug/L mn - 5) CHLOROMETHANE 5.47 50 611729 10.85 ug/L 99 —mtn 6) VINYL CHLORIDE 5.59 62 273752 12.42 ug/L 100 7) BROMOMETHANE 6.58 94 370463 11.22 ug/L 98 8) CHLOROETHANE 6.73 64 326273 10.24 ug/L 96 9) TRICHLOROFLUOROMETHANE 7.29 101 660406 10.48 u§/L 98 11) 1,1,2-Trichloro-1,2,2-trif 8.18 101 391286 8.30 ug/L 96 12) ACETONE 8.25 43 125282 9.84 ug/L 98 13) 1,1-DICHLOROETHENE 8.62 61 900383 10.13 ug/L 99 14) METHYLENE CHLORIDE 9.61 49 1092180 10,25 ug/L 95 15) METHYL TERT BUTYL ETHER 9.93 73 1019536 8.63 ug/L 96 16) TRANS-1,2-DICHLOROETHENE 10.27 61 1099760 9.67 ug/L 94 17) 1,1-DICHLOROETHANE 11.18 63 1323142 9.84 ug/L 97 -th 18) 2-BUTANONE (MEK) 12.00 43 323113 11.14 ug/L 98 nute 19) 2,2-DICHLOROPROPANE 12.40 77 881414 8.17 ug/L 99 -l. 20) CIS-1,2-DICHLOROETHENE 12.48 96 747499 9.74 ug/L 97 21) CHLOROFORM 12.81 83 1355186 10.03 ug/L 99 22) BROMOCHLOROMETHANE 13.20 49 643854 10.02 ug/L 95 23) 1,2-DICHLOROETHANE 14.54 62 912977 10.04 ug/L 98 -andsr 26) 1,1,1-TRICHLOROETHANE 13.72 97 998450 9.73 ug/L 98 -lim 27) 1,1-DICHLOROPROPENE 14.03 75 1037844 10.14 ug/L 100 28) CARBON TETRACHLORIDE 14.29 117 806958 9.67 ug/L 100 29) BENZENE 14.64 78 2623544 9.87 ug/L 30) TRICHLOROETHENE 15.91 95 810149 10.20 ug/L 99? 31) 1,2-DICHLOROPROPANE 16.26 63 778216 10.36 ug/L 99 32) DIBROMOMETHANE 16.94 174 350480 9.83 ug/L 98 33) BROMODICHLOROMETHANE 16.78 83 979748 10.19 ug/L 98 34) 2-CHLOROETHYL VINYL ETHER 17.27 63 289850 10.44 ug/L 95 (#) = qualifier out of range (m) = manual integration 0208C10D.D HP021102.M Mon Feb 11 16:22:02 2002 Page 1 —

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