VOC analysis results, sample AE02575, Feb 8 2002

NYC 9/11 Public Portal Document at

md Data File C: \HPCHEM\ 1 \DATA\ 0 2 FEB 08\0208R5A.D Vial: 2 Acq On 8 Feb 2002 6:38 pm Operator: 201-wb Sample ref 5 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P -t Quant Time: Feb 11 16:22 2002 Quant Results File: HP021102 .RES

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Feb 11 15:54:13 2002 Response via : Initial Calibration mmdn DataAcq Meth : HP020502

Internal Standards R.T. Qlon Response Cone Units Dev(Min) t - “ - -------- on 1) 1,4-DIFLUOROBENZENE 15.13 114 2105266 5.00 ug/L 0.02 24) CHLOROBENZENE-D5 21.78 117 1996586 5.00 ug/L 0.02 52) 1,4-DICHLOROBENZENE-D4 26.95 152 898368 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.36 65 780705 4.87 ug/L 0.02 Spiked Amount 5.000 Recovery = 97.40% 3) 4-BROMOFLUOROBENZENE 24.35 174 716198 4.53 ug/L 0.00 - Spiked Amount 5.000 Recovery = 90.60% 25) TOLUENE-D8 18.47 98 2550493 5.15 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.00% do hi =l Target Compounds Qvalue 5. 4) DICHLORODIFLUOROMETHANE 4.89 85 422451 5.03 ug/L 99 5) CHLOROMETHANE 5.47 50 349001 5.29 ug/L 96 nde 6) VINYL CHLORIDE 5.61 62 169783 5.73 ug/L 100 7) BROMOMETHANE 6.60 94 200085 5.33 ug/L 96 8) CHLOROETHANE 6.75 64 177010 4.75 ug/L 95 = 9) TRICHLOROFLUOROMETHANE 7.30 101 358462 5.00 ug/L 100 12) ACETONE 8.29 43 68027 4.70 ug/L 93 13) 1,1-DICHLOROETHENE 8.64 61 477409 4.72 ug/L 96 7 “ .nnii 14) METHYLENE CHLORIDE 9.63 49 630740 5.21 ug/L 94 m 15) METHYL TERT BUTYL ETHER 9.94 73 527125 3.92 ug/L 93 — 16) TRANS-1,2-DICHLOROETHENE 10.31 61 601008 4.65 ug/L 97 — 17) 1,1-DICHLOROETHANE 11.20 63 731994 4.79 ug/L 99 — 18) 2-BUTANONE (MEK) 12.03 43 213638 6.48 ug/L 100 19) 2,2-DICHLOROPROPANE 12.41 77 588942 4.80 ug/L 98 20) CIS-1,2-DICHLOROETHENE 12.50 96 438318 5.02 ug/L 100 21) CHLOROFORM 12.83 83 777771 5.06 ug/L 98 2 2) BROMOCHLOROMETHANE 13.22 49 350813 4.80 ug/L 96 23) 1,2-DICHLOROETHANE 14.56 62 504681 4.88 ug/L 100 to 26) 1,1,1-TRICHLOROETHANE 13.74 97 578027 5.19 ug/L 97 27) 1,1-DICHLOROPROPENE 14.05 75 614539 5.53 ug/L 99 28) CARBON TETRACHLORIDE 14.31 117 467828 5.17 ug/L 100 — 29) BENZENE 14.66 78 1546888 5.36 ug/L 99 — 30) TRICHLOROETHENE 15.93 95 491038 5.69 ug/L 99 — 31) 1,2 -DICHLOROPROPANE 16.28 63 452464 5.55 ug/L 98 — 32) DIBROMOMETHANE 16.96 174 186675 4.82 ug/L 96 —= 33) BROMODICHLOROMETHANE 16.80 83 553168 5.30 ug/L 100 — 34) 2-CHLOROETHYL VINYL ETHER 17.29 63 136755 4.54 ug/L 100 — 35) METHYL ISO-BUTYL KETONE 17.36 58 71540 4.79 ug/L 100 -

(#) = qualifier out of range (m) = manual integration 0208R5A.D HP021102.M Mon Feb 11 16:22:41 2002 Page 1• h —

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