SB1524 volatile analysis results, sample AEO1636, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\02JAN31\1638.D Vial: 19 Acq On : 31 Jan 2002 10:51 pm Operator: 206-bh Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Benzenesulfonic acid, hydrazid Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.14 0.56 ug/L 47299 1,4-DIFLUOROBENZENE 14.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzenesulfonic acid, hydrazide 172 C6H8N2O2S 000080-17-1 83 2 2,4-Hexadiyne 78 C6H6 002809-69-0 74 3 1,5-Hexadiyne 78 C6H6 000628-16-0 74 4 1,3,5,7-Cyclooctatetraene 104 C8H8 000629-20-9 64 Abundance Scan 126 (5.145 min): 1638.D (-) m/z 78.10 100.00%

M 49 62 78 8000 207 6000

4000 91 “W4.80 5.00 5.20 5.40 m/z 62.10 87.75% niz-> :20 30 40 53 60 70 80 90 100110120130140150160170180190200210 Abundance #68305: Benzenesulfonic acid, hydrazide 78 48

5000 4.80 5.00 5.20 5.40..... 64 m/z 49.10 87.46% ...... |.... .. 94.310 125.142..... ......... 20 30"40‘ 5o‘ 60 70* 80" 90 100110120130140150160170180190 200 210 niz—> Abundance #402:2,4-Hexadiyne 73 i i 1Li i i । i > i > j : i i T-1 i T-1 I । i 4.80 5.00 5.20 5.40 51 m/z 207.10 63.60% 5000

m 37 ............. lj 63 I}, t -I1,'Jl-I ............. . II iz—> 20 30 40 50 60 70 80 90 100 110 120130140150160170180190 200 210' Abundance 33 78 #405:1,5-Hexadiyne • • i • ■ 4.80 5.00 AA 5.20 5.40 m/z 45.10 52.07% 52 5000

27 63

n/z—> 20 30 40 53 60 70 80 90 100110120130140150160170180190200210 4.80 5.00 5.20 5.40

1638.D MDLVOA.M Tue Feb 19 16:50:17 2002 Page 1

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