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SB1524 volatile analysis results, sample AEO1636, Jan 2002

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Laboratory report detailing SB1524 analysis of sample AEO1636 for volatile organic compounds including acetone and vinyl chloride on January 28, 2002.

NYC-WTC_000019175–000019231

Folder label: “524 1/28/02 AND 1/31/02

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Scanned page image, NYC-WTC_000019205
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02JAN28\1637.D Vial: 4 Acq On : 28 Jan 2002 6:55 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : January 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Hydroxypethidine Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.62 1.45 ug/L 884501 1,4-DIFLUOROBENZENE 15.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Hydroxypethidine 263 C15H21NO3 000468-56-4 94 2 Nonanoic acid, 9-phenyl-, methyl es 248 C16H24O2 024197-55-5 91 3 Propanedinitrile, (2-methylpropylid 120 C7H8N2 013134-03-7 91 4 4(1H)-Pyrimidinone, 2-(methylthio)- 142 C5H6N20S 005751-20-2 91 Abundance Scan 96 (5.621 min): 1637.D (-) m/z 78.10 100.00%| 78

5000 45 94 uaw/ywp I , .. 134 173 201 227244 10 IW II il I H l 11755 I J 261 281299 l ,261 298

m/z-> Abundance pTT JMInM 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #36410: Hydroxypethidine 5.20 5.40 5.60 5.80 6.00 m/z 63.20 66.49

i[ 35

A 5000 71 5.20 5.40 5.60 5.80 6.00 | 140 263 m/z 45.10 58.31% 189 p-n- 156 bl.. .X. ... m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #33568: Nonanoic acid, 9-phenyl-, methyl ester 91

5000 74

31 .1117133.. „fls. 248 mn rAWW .. ।. I.. ।. 1111111111 ' 11 • ‘ ■ I ■ ‘ ■ I'" ‘ I ■ ■ ■ ‘ I " m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #3745: Propanedinitrile, (2-methylpropylidene)- T-rpr-n-rpr-r 42 5.20 5.40 5.60 5.80 6.00 | m/z 93.90 56.92% 105 5000 78

TpT-rrpTTpTn-rTp-rrrp-rrTp-rTTpT-rp-rTTTp-rTp-rT^^ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 5.20 5.40 5.60 5.80 6.00

1637.D HP021702.M Tue Feb 19 16:57:28 2002 Page 1

NYC-WTC_000019205

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NYC-WTC_000019205Source: NYC Law Department, mirrored locally

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