GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC2101\30312.D Vial: 13 Acq On : 22 Dec 2001 6:33 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.77 ug/1 1129200 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Silane, tramethyl- 88 C4H12Si 000075-76-3 9 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 l-Bu^anamine, 3-methyl- 87 C5H13N 000107-85-7 9 Abundance Scan 279 (7.608 min): 30312.D (-) m/z 73.00 100.00% 73

5000 43 . .. ... 38,441, 50 87 103 ,67,^ Hr ’I***1***I*** 7.20 7.40 7.60 7.80 8.00 ' ■ ' i • ■ ' ■ i ' ■ • ■ i ‘ ■ ’I** m/z 43.05 30.55% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 7.20 7.40 7.60 7.80 8.00 45 m/z 44.95 11.10% 15 , J 53 59 | 88 /l m/z-> 10 20 30 40 50 60 ■ ■ i ■ 1 • ■ i ■ 1 ■ ‘ i 1 ■ • ■ i ■ ■ ■ ■ i • ‘ 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane 2-methyl- 73 1*3 Tu r i i । । । । > |~n-r 1 i ■ • 7.20 7.40 7.60 7.80 8.00 5000 43 m/z 41.00 10.70% 58 27 87 TII— —BnmmT ‘ i • i ‘ 1 i 1 • • ■ i ■ 1 • ■ i • ■ ■ ■ i ■ • ‘ ‘ i ■ ■ ■ ■ i • ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide ITT I . q r rt i । , j . , . i । j , 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.0k0 6.66% 5000 44 58 15 1 ■ ■ lip ■> t ■ • i • ‘ ■ 1 i ' 1 ■ ■ i ■ • ■ ‘ i ■ ■ • ■ i ■ • ■ • i 1 1 .................. miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30312.D GCMS1126.M Wed Jan 02 10:16:08 2002 Page 1

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