GCMS analysis results for sample AD30426, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\HPCHEM\l\DATA\DEC2701\30426.D Vial: 23 Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.61 4.46 ug/1 1480910 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 280 (7.612 min): 30426.D (-) m/z 72.95 100.00% 73

5000 43 ............................ 87 7.20 7.40 7.60 7.80 8.00 38 I, I 50 5.5, 60 67, 1 , 103 : ■ • 1 ' 1 1 ■ i ■ ‘ ‘ ' I ' TIIIm rn/z 43.0.0 31.03% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 1**4*1*"*1****1*‘‘*I‘* 7.20 7.40 7.60 7.80 8.00 45 m/z 45.0.0 11.36% 15 , . 53 59 88......................... ■ 1 i ■ ■ i ■ ■ • ■ i 1 ' ' ■ i । 1 ■ • i ■ 1 ■ 'i ■ ■ ■ 1 i 1

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902:1,3-Dioxolane, 2-methyl 73 P" ‘ 14 f ‘ 4" » j l . . . J. i . . 1 . . 7.20 7.40 7.60 7.80 8.00 5000 43 m/z 41.0.5 11.25% 58 87 27 । , ■ 1 । । । । l ■ ■ । • l'i U* ri ————— 1 ■ ■ i 1 ■ ■ ‘ i ■ ‘ ■ i ■ ■ 1 • i • ■

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide mn gri , mmm F| "I "P 30 7.20 7.40 7.60 i7.80 8.00 73 m/z 71.00 6.81% 5000 44 58

15 1211.1 ■ lie 1aaa 1141*1**1*1 CT4 i -i i । । rr iJ| i i ITFPrrr । ■ r miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30426.D GCMS1126.M Wed Jan 02 11:07:39 2002 Page 1

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