GCMS sample analysis results, Jan 2002

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Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30260 conducted on January 9, 2002.

NYC-WTC_000019081–000019089

Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2101\30250.D Vial: 9 Acq On : 22 Dec 2001 2:39 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 27 9:25 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GOMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 823225 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3167222 20.00 ug/1 -0.03 17) Acenaphthene-dl0 20.56 164 1602989 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 2339210m 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1462277 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 918894 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.06 235 138883 4.10 ug/mL -0.01 Spiked Amount 5.000 Recovery = 82.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.21 74 173 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichiorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichiorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.32 128 864 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.11 165 310 N.D. 25) Diethylphthalate 22.13 149 385 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30250.D GCMS1126.M Thu Dec 27 09:58:32 2001 Page 1

NYC-WTC_000019083

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