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GCMS calibration table, sample AD31129, Jan 2002

Machine-extracted title · confidence 100%

GCMS calibration table for sample AD31129 listing deuterated standards and retention times from January 10, 2002.

NYC-WTC_000018962–000018971

Folder label: “GCMS X 12/21/01 A 1/10/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C: \HPCHEM\ 1 \DATA\ JANO 902\31129A.D Vial: 26 Acq On : 10 Jan 2002 3:31 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

. peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.465 260 264 272 rBV 300856 755205 9.82% 1.961% 2 7.566 272 275 301 rVB 330063 1026104 13.34% 2.664% 3 11.523 701 706 726 rBV 2266234 5846494 76.02% 15.180% 4 14.166 989 994 1000 rVB 52049 104254 1.36% 0.271% 5 15.121 1093 1098 1117 rBV 3582432 7454004 96.92% 19.353%

6 20.391 1666 1672 1691 rBV 3754667 7690487 100.00% 19.967% 7 24.806 2147 2153 2165 rBV2 3326082 7212116 93.78% 18.725% 8 24.953 2165 2169 2182 rVB2 24042 88403 1.15% 0.230% 9 29.883 2701 2706 2713 rBV 316109 636981 8.28% 1.654% 10 32.839 3021 3028 3049 rBV2 2002567 4614847 60.01% 11.982%

11 36.906 3464 3471 3498 rBV2 1112372 3086492 40.13% 8.014%

Sum of corrected areas: 38515387

31129A.D GCMS0103.M Wed Feb 06 09:21:07 2002

NYC-WTC_000018965

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NYC-WTC_000018965Source: NYC Law Department, mirrored locally

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