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GCMS analysis results for sample AD28860, Dec 16 2001

Machine-extracted title · confidence 100%

Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.

NYC-WTC_000018817–000018829

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01

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Scanned page image, NYC-WTC_000018822
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NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File : M:\INSTRU~1\209\DATA\DEC2701\29735.D Vial: 18 Acq On : 29 Dec 2001 3:45 pm Operator: 209 GALOS Sanpl e : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.611 276 280 310 rBV 322716 1116753 13.27% 2.656% 2 11.127 657 663 672 rBV 40139 106666 1.27% 0.254% 3 11.678 718 723 754 rBV 2168969 6424020 76.35% 15.280% 4 14.304 1004 1009 1016 rBV 113577 257801 3.06% 0.613% 5 15.277 1110 1115 1135 rBV 2970648 7791040 92.60% 18.532%

6 17.453 1347 1352 1361 rVB 136213 287077 3.41% 0.683% 7 20.280 1654 1660 1666 rBV 74186 157332 1.87% 0.374% 8 20.565 1684 1691 1715 rBV 3318158 8413735 100.00% 20.013% 9 24.980 2166 2172 2213 rBV2 2679107 7862071 93.44% 18.701% 10 30.066 2720 2726 2737 rBV 375022 851013 10.11% 2.024%

11 33.022 3041 3048 3075 rBV2 1898948 5370299 63.83% 12.774% 12 37.117 3487 3494 3524 rBV 974364 3404058 40.46% 8.097%

Sum of corrected areas: 42041865

29735.D GCMS1126.M Tue Jan 29 14:26:51 2002

NYC-WTC_000018822

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NYC-WTC_000018822Source: NYC Law Department, mirrored locally

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