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GCMS results for unknowns, sample AD30485, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD30485 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.

NYC-WTC_000018870–000018881

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01

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Scanned page image, NYC-WTC_000018875
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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : M:\INSTRU~1\209\DATA\DEC2101\30485.D Vial: 23 Acq On : 23 Dec 2001 6:12 am Operator: 209 GALOS Sample : gc/ms scan 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 276 280 292 rBV 302004 888617 11.66% 2.321% 2 7.750 292 295 308 rVB2 43369 171896 2.25% 0.449% 3 11.358 684 688 692 rBV2 40315 95165 1.25% 0.249% 4 11.440 693 697 712 rVB 46417 163412 2.14% 0.427% 5 11.670 717 722 747 rBV 2105520 5910545 77.52% 15.437%

6 15.278 1109 1115 1134 rBV 3122089 7170515 94.05% 18.728% 7 20.556 1683 1690 1716 rBV 3309767 7624166 100.00% 19.913% 8 24.972 2165 2171 2186 rBV2 2815696 6903082 90.54% 18.029% 9 27.001 2386 2392 2401 rBV 54060 145751 1.91% 0.381% 10 30.058 2719 2725 2733 rBV 354631 777419 10.20% 2.030% 11 33.014 3040 3047 3066 rBV 1942246 4870920 63.89% 12.722% 12 37.108 3485 3493 3518 rBV2 1132458 3566639 46.78% 9.315%

Sum of corrected areas: 38288127

30485.D GCMS1126.M Tue Jan 29 14:18:21 2002

NYC-WTC_000018875

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NYC-WTC_000018875Source: NYC Law Department, mirrored locally

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