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GCMS results for unknowns, sample AD26477, Dec 2001

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD26477 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.

NYC-WTC_000018923–000018933

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : M:\INSTRU~1\209\DATA\DEC2701\26477.D Vial: 10 Acq On : 27 Dec 2001 8:54 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 276 280 314 rBV 417819 1267251 15.15% 3.008% 2 11.128 658 663 673 rBV 39083 92753 1.11% 0.220% 3 11.679 718 723 756 rBV 2309815 6158237 73.63% 14.619% 4 14.304 1003 1009 1016 rBV 79240 167865 2.01% 0.398% 5 15.277 1110 1115 1135 rBV 3157027 7615039 91.04% 18.077%

6 20.556 1684 1690 1729 rBV 3437549 8364173 100.00% 19.855% 7 24.981 2165 2172 2185 rBV2 3241721 7810034 93.37% 18.540% 8 27.010 2388 2393 2403 rBV 30019 107498 1.29% 0.255% 9 30.058 2720 2725 2737 rBV 494602 1150347 13.75% 2.731% 10 33.023 3041 3048 3075 rBV 2114378 5621742 67.21% 13.345%

11 37.117 3486 3494,3518 rBV2 1124913 3771328 45.09% 8.952%

Sum of corrected areas: 42126267

26477.D GCMS1126.M Tue Jan 29 14:21:53 2002

NYC-WTC_000018928

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NYC-WTC_000018928Source: NYC Law Department, mirrored locally

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