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GC/MS analysis results for sample AD30906, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.

NYC-WTC_000018650–000018663

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30906.D Vial: 42 Acq On 2 Jan 2002 4:39 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Silane, [1,2,3-benzenetriyltri Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.45 0.57 ug/1 191111 Naphthalene -d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, [1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 22 2 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OS13 000000-00-0 9 4 2H-1,4-Ben: diazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 9 Abundance Scan 1352 (17.455 min): 30906.D (-) m/z 73.00 100.00%| 73

5000 341 /. 147 T T 45 429 17.20 17.40 17.60 17.80

miz-> why 117 179 207 TITTTT *mt apaponposho 251 281 311 L | [ 40 60 80 100120140160180200220240260280300320340360380400420 m/z 341.00 28.55 Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trlmethyl- 73 239 5000 342 •11 ■ • ■ ■ । • • ■ ■ ।11'111 ■ 17.20 17.40 17.60 17.80 45 m/z 147.10 14.32 133 ...................................... ....... ...... ................ ........................ ....... | mg 179 211 ‘ ‘1’411444 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 ' Abundance #567 14. 1.1.1 .5,7.7.7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 ................ \.................. • ' । 1 ■ 1 1 1B.4 । । । i > । > p । 147 17.20 17.40 17.60 17.80 5000 I 267 m/z 342.00 9.92% 355 429 45 207 ! . ............ ....... ..................................... ...................................1,1 ........ , Wz-> 40 60 80 100120140160180 200 220240 260 280 300 320 340 360 380 400 420 ' Abundance 73 #48317:4-Amino-5-lmidazole carboxamide, tris(trimethylsily T 4 T 17.20 17,40 17.60 17.80 m/z 325.00 9.46% 327 5000 237 45 m.......... mPna 147172 212 ........................................ 1 ' i 1 ■ ■ ■ i 1 • ' • I 1 1 1 1 I ' 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 ’ 17.20 17.40 17.60 17.80

30906.D GCMS1126.M Fri Jan 25 11:32:47 2002 Page 4

NYC-WTC_000018660

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