NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30906.D Vial: 42
Acq On 2 Jan 2002 4:39 am Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Silane, [1,2,3-benzenetriyltri Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 0.57 ug/1 191111 Naphthalene -d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Silane, [1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 22
2 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16
3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OS13 000000-00-0 9
4 2H-1,4-Ben: diazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 9
Abundance Scan 1352 (17.455 min): 30906.D (-) m/z 73.00 100.00%|
73
5000
341 /.
147 T T
45 429 17.20 17.40 17.60 17.80
miz->
why 117 179 207
TITTTT *mt apaponposho
251 281 311 L |
[
40 60 80 100120140160180200220240260280300320340360380400420
m/z 341.00 28.55
Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trlmethyl-
73
239
5000 342 •11 ■ • ■ ■ । • • ■ ■ ।11'111 ■
17.20 17.40 17.60 17.80
45 m/z 147.10 14.32
133
...................................... ....... ...... ................ ........................ .......
| mg 179 211
‘ ‘1’411444
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 '
Abundance #567 14. 1.1.1 .5,7.7.7-Heptamethyl-3,3-bis(trimethylsiloxy)t
73 ................ \..................
• ' । 1 ■ 1 1 1B.4 । । । i > । > p ।
147 17.20 17.40 17.60 17.80
5000
I 267 m/z 342.00 9.92%
355 429
45 207
! . ............ ....... ..................................... ...................................1,1 ........ ,
Wz-> 40 60 80 100120140160180 200 220240 260 280 300 320 340 360 380 400 420 '
Abundance
73
#48317:4-Amino-5-lmidazole carboxamide, tris(trimethylsily T 4 T
17.20 17,40 17.60 17.80
m/z 325.00 9.46%
327
5000
237
45
m..........
mPna 147172
212 ........................................
1 ' i 1 ■ ■ ■ i 1 • ' • I 1 1 1 1 I ' 1
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 ’ 17.20 17.40 17.60 17.80
30906.D GCMS1126.M Fri Jan 25 11:32:47 2002 Page 4
NYC-WTC_000018660
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