GC/MS analysis results for sample AD30904, Jan 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30904.D Vial: 44 Acq On 2 Jan 2002 6:35 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************************************************** ***************** Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

21.10 0.69 ug/1 219475 Acenaphthene-dl0 20.56

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 4-ethoxy-, ethyl este 194 C11H14O3 023676-09-7 97 2 1-Cyclopentene-1-propanoic acid, .b 168 C10H16O2 061833-30-5 80 3 1-Butanone, 4-chloro-1- (4-hydroxyph 198 C10H11C1O2 007150-55-2 43 4 Benzoic acid; ethoxy-, ethyl ester 194 C11H1403 075333-22-1 43 Abundance Scan 1749 (21.098 mln): 30904.D (-) rn/z 120.95 100.00% 121

5000 149 138 194 39 * 65 93 166 20*80 21.00 21.20 21.40 m In 99. ., Ik ,,. #,84 ■ Al me 109 i ... * ..... # , ■ ■ । ■! ■. „ t, ■,, t. lb .,, ■ ■ 76 84—all| ...9Y m/z 149.00 44.84% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #69400: Benzoic add, 4-ethoxy-, ethyl ester i 121

149 _______ _ 5000 194 65 138 20.80 21.00 21.20 21.40 93 166 m/z 194.05 28.40% 50 I''' ‘ I ‘ ‘' 1'' ‘' I ‘‘ 76 1 ,1 1111111 11 l‘i 111111111 > 11 |'H i. p ri 1 j 111 II"’ 11111111 | 11 11 1111 111 1111 i miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #14561: 1-Cyclopentene-1-propanoic acid, .beta.-methyl-, me 58 79 95 121 8000 T 20.80 21.00 21.20 21.40 109 6000 m/z 138.05 26.81% 4000 150 ‘I*‘‘I9BBI—*‘I‘2‘/***/***7‘*IIISWUISNTAIAASSASEIAI+ ,-| 111111111111 > 11111 168 m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 .Abundance #22266:1-Butanone, 4-chloro-1-(4-hydroxyphenyl)- PPTA 121 20.80 21.00 21.20 21.40 m/z 65.05 19.82% 5000 136 I ' 65 93 41 53 J 77 | , 162 198 j i«■»।»i * .|-r. >. | sli i p i l'i p 11 1111 11 p 11111 111111 r 111 il'i | 11! 1111 1 > |I! myaalip 111 ip 11 11111 M,.A ,TY miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40

30904.D GCMS1126.M Fri Jan 25 11:30:00 2002 Page 6

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