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GCMS analysis results for sample AD31465, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31465 conducted on February 11, 2002.

NYC-WTC_000018385–000018394

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018390
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File : C:\HPCHEM\1\DATA\JAN1602\31465.D Vial: 28 Acq On : 17 Jan 2002 3:01 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.448 258 262 281 rBV 407328 1134203 15.56% 2.962% 2 11.276 675 679 687 rVB 28530 77095 1.06% 0.201% 3 11.496 698 703 727 rBV 2159181 5728222 78.60% 14.959% 4 15.095 1089 1095 1113 rBV 3451926 7075374 97.09% 18.478% 5 20.355 1662 1668 1682 rBV 3414332 7287486 100.00% 19.031%

6 24.771 2143 2149 2162 rBV2 3129503 6863011 94.18% 17.923% 7 29.848 2697 2702 2709 rBV 401497 827358 11.35% 2.161% 8 32.804 3017 3024 3044 rBV2 2244049 5244566 71.97% 13.696% 9 36.870 3460 3467 3493 rBV 1441985 4054398 55.64% 10.588%

Sum of corrected areas: 38291713

31465.D GCMS0103.M Thu Feb 07 12:41:10 2002

NYC-WTC_000018390

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NYC-WTC_000018390Source: NYC Law Department, mirrored locally

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