NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
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Data File : C:\HPCHEM\1\DATA\JAN1602\31434.D Vial: 21
Acq On : 17 Jan 2002 7:11 am Operator: 209 GALOS
Sample : gc/ms scan 12/28 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 7 11:49 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon Jan 07 10:31:02 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.50 152 778316 20.00 ug/1 -0.03
10) Naphthalene-d8 15.09 136 3053275 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.36 164 1541957 20.00 ug/1 -0.03
29) Phenanthrene-diO 24.78 188 2126822 20.00 ug/1 -0.03
38) Chrysene-dl2 32.80 240 1302813 20.00 ug/1 -0.04
44) Perylene-dl2 36.87 264 839588 20.00 ug/1 -0.03
System Monitoring Compounds
37) 2,4-DDD 29.85 235 96942 3.97 ug/mL -0.22
Spiked Amount 5.000 Recovery = 79.40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 12.86 77 106 N.D.
12) 1sophorone 13.32 82 106 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.15 128 1284 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachiorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
22) Acenaphthylene 0.00 152 0 N.D.
23) Ac enapht hene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.75 165 109 N.D.
25) Diethylphthalate 21.88 149 1709 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
31434.D GCMS0103.M Thu Feb 07 11:49:46 2002 Page 1
NYC-WTC_000018317
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