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GCMS analysis results for sample AD30985, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\ 1\DATA\DEC3101\30985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.43 ug/1 917358 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penta: , 3-methyl- 102 C6H140 000077-74-7 33 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 N-E'thyl formamide 73 C3H7NO 000627-45-2 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 280 (7.612 min): 30985.D (-) m/z 73.00 1 00.00% 73

5000 43 i ■ ' ■ ■ i 1 1 1 1 i 1 ■ 1'1Tr * । • 7.20 7.40 7.60 7.80 8.00 mpmmpmm .1 1 55 i hp87 103 207 II1111.(.11.।।।1(....।...h....।.11.1(।।. m/z 43.05 32.86% m/z-> 10 2030405060 70 8090 100110120130140150160170180190200210 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.20 7.40 7.60 7.80 8.00 45 55 87 m/z 45.05 11.62%

m/z-> 27 1 , 4 ■ I,.... ,1............................................................... 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62902: 1.3-Dioxolane, 2-methyl- 73 ' nmmOTrrrmTr 7.20 7.40 7.60 7.80 8.00 5000 43 m/z 41.05 11.55% .......... ........ .. 58 27 87 ... I.... 1..1.1.H11Hi.11..I!... 111...|.1|||1.... 11m 11U111 r m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #292: N-Ethylformamide I I I » « l” J > I ' I • I J • » « • I • » ' 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.00 7.25% 5000 44 58

miz-> .15 mhp [ .... j 11 . I I 11 j i 11 . | ... I । 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 । । I।। । । I 11 l 1 ! J!! I ! | l t 1 17644142411844 1 TTv 7.20 7.40 7.60 7.80 8.00

30985.D GCMS1126.M Wed Jan 23 08:56:59 2002 Page 1

NYC-WTC_000018269

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NYC-WTC_000018269Source: NYC Law Department, mirrored locally

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