GCMS DFTPP calibration verification, Jan 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\DEC31O1\DFTPP1.D Vial: 1 Acq On 1 Jan 2002 11:13 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP1.D

1e+07 8000000

6000000

4000000

U 2000000 24.40 24^60 24.80 25^00 25.20 25.40 2a0 25.80 28*66 236720 26.60 24460 27.20 27*40 27.60 28 28*00 ' 01 Time-> Abundance Average of 26.211 to 26.293 min.: DFTPP1 .D 198 600000

400000 69 127 51 255 442

110 200000 275 224 93 148 167 180 0 l . >i *' +* 4**1444* **l* H 4H +r-ree • 38 1411/4248.47 nJ. । 4.296310323336 r। 352385 3S3 403 423 । i. .i j-i-i ri । rrt । 11 । । i |-i । । । IT i I TT11 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.211 to 26.293 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 47.9 327188 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 58.5 399652 PASS 70 69 0.00 2 0.0 65 PASS 127 198 40 60 53.7 366996 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 683025 PASS 199 198 5 9 6.7 46057 PASS 275 198 10 30 20.5 140101 PASS 365 198 1 100 2.7 18430 PASS 441 443 0.01 100 94.1 62255 PASS 442 198 40 110 49.8 340466 PASS 443 442 17 23 19.4 66137 PASS

DFTPP1.D GCMS1126.M Fri Jan 18 08:38:14 2002

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