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GCMS analysis results for sample AD28968, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28968 conducted on January 9, 2002.

NYC-WTC_000018026–000018035

Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01

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Scanned page image, NYC-WTC_000018031
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1201\28968.D Vial: 31 Acq On : 13 Dec 2001 7:15 am Operator: 209 GALOS Sample : gc/ms scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.603 275 279 312 rVB 287252 874489 9.81% 1.950% 2 11.348 683 687 692 rBV 38250 94378 1.06% 0.210% 3 11.431 692 696 717 rVB 46091 157170 1.76% 0.351% 4 11.669 717 722 741 rBV 2462407 6271903 70.35% 13.988% 5 15.277 1109 1115 1133 rBV 3711978 8092669 90.78% 18.048%

6 20.556 1683 1690 1707 rBV 4019628 8914879 100.00% 19.882% 7 24.972 2165 2171 2183 rBV2 3583021 8118433 91.07% 18.106% 8 25.119 2183 2187 2197 rVB3 36434 105520 1.18% 0.235% 9 30.048 2718 2724 2733 rBV 457199 942705 10.57% 2.102% 10 33.014 3039 3047 3061 rBV2 2545664 6201579 69.56% 13.831%

11 33.289 3072 3077 3088 rVB 54780 151651 1.70% 0.338% 12 37.108 3484 3493 3509 rBV2 1619156 4913889 55.12% 10.959%

Sum of corrected areas: 44839265

28968.D GCMS1126.M Tue Jan 08 09:29:20 2002

NYC-WTC_000018031

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NYC-WTC_000018031Source: NYC Law Department, mirrored locally

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