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GCMS analysis results for sample AD25946, Jan 2002

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Laboratory report noting detection of 1,1,2,2-Tetrachloroethane in a water sample with no other non-target compounds.

NYC-WTC_000017997–000018004

Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\25946.D Vial: 25 Acq On 1 Jan 2002 10:15 am perator: 209 GALOS Sample gems scan 12/14a nst : GC/MS 209 Mise uibiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 14:41 2002 Qu suits File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (R Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 866694 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3405092 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1752328 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 2426945m 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1518340 20.00 ug/1 0.00 44) Perylene-dl2 37.11 264 838643 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 114592 4.29 ug/mL 0.00 Spiked Amount 5.000 Recovery = 85.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.34 77 105 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 787 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.21 165 219 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 25946.D GCMS1126.M Fri Jan 18 15:20:45 2002 Page 1

NYC-WTC_000017998

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NYC-WTC_000017998Source: NYC Law Department, mirrored locally

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