NYC-WTC_000017981
Laboratory notes regarding GCMS scan results and recovery rates for sample AD25874 dated January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS analysis results, sample AD26011, January 2002
Machine-extracted title · confidence 75%Gas chromatography-mass spectrometry analysis of sample AD26011 from January 18, 2002, detecting 2-(2-ethoxyethoxy)ethanol and 2-ethoxybutane with no blank contamination.
NYC-WTC_000017989–000017996Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) 4 a Data.File C:\HPCHEM\l\DATA\DEC3101\26011.D I Vial: 20 Acq On 1 Jan 2002 5:25 am _ — Vo Operator: 209 GALOS Sample gems scan 12/14a 115 \ Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 14:03 2002 Qua; suits File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.68 152 747055 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 2910065 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 1473022 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 1970751m 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1186285 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 665722 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.07 235 116488 5.38 ug/mL 0.00 Spiked Amount 5.000 Recovery = 107.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.28 74 189 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 632 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Ac enapht hylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.00 165 564 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 26011.D GCMS0103.M Tue Jan 15 14:03:30 2002 Page 1
NYC-WTC_000017990
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