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GCMS analysis results, sample AD26011, January 2002

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Gas chromatography-mass spectrometry analysis of sample AD26011 from January 18, 2002, detecting 2-(2-ethoxyethoxy)ethanol and 2-ethoxybutane with no blank contamination.

NYC-WTC_000017989–000017996

Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) 0 Data File C:\HPCHEM\1\DATA\DEC3101\26011.D Vial: 20 Acq On 1 Jan 2002 5:25 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 14:03 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001. Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.06 178 180 N.D. 3 4) Anthracene 25.06 178 180 N.D. 35) Di-n-butylphthalate 27.07 149 2461 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 2673 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 4268 N.D. 43) Chrysene 33.02 228 2673 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 4 7) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.13 252 2371 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 26011.D GCMS0103.M Tue Jan 15 14:03:34 2002 Page 2

NYC-WTC_000017991

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NYC-WTC_000017991Source: NYC Law Department, mirrored locally

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