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GCMS comments for sample AD25874, Jan 2002

Machine-extracted title · confidence 100%

Laboratory notes regarding GCMS scan results and recovery rates for sample AD25874 dated January 18, 2002.

NYC-WTC_000017981–000017988

Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01

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Scanned page image, NYC-WTC_000017985
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

.LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC3101\25874.D Vial: 19 Acq On 1 Jan 2002 4:27 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.609 275 279 308 rBV 275411 948021 15.64% 3.189% 2 11.676 717 722 747 rBV 1660542 4503737 74.29% 15.152% 3 15.274 1109 1114 1134 rBV 1957369 5548381 91.52% 18.667% 4 20.562 1684 1690 1718 rBV 2179262 6062229 100.00% 20.396% 5 24.987 2166 2172 2219 rBV2 1603166 5732685 94.56% 19.287%

6 30.073 2720 2726 2738 rBV 243147 609610 10.06% 2.051% 7 33.029 3041 3048 3075 rBV2 1214816 3851685 63.54% 12.958% 8 37.123 3487 3494 3521 rBV 600885 2466931 40.69% 8.300%

Sum of corrected areas: 29723279

25874.D GCMS1126.M Tue Jan 15 14:45:46 2002

NYC-WTC_000017985

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NYC-WTC_000017985Source: NYC Law Department, mirrored locally

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