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GCMS calibration data sheet, Dec 2001

Machine-extracted title · confidence 95%

Document showing calibration results for GCMS analysis of volatile organic compounds on December 31, 2001.

NYC-WTC_000017883–000017893

Folder label: “GCMS X 12/14/01 A 12/31/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC3101\LBA.D Vial: 5 Acq On : 31 Dec 2001 2:51 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 11:12 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title •: 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.05 178 179 N.D. 34) Anthracene 25.08 178 117 N.D. 35) Di-n-butylphthalate 27.04 149 3678 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.52 149 1628 N.D. 41) Benzo(a)anthracene 33.02 228 4243 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 19034 0.28 ug/1 92 43) Chrysene 33.11 228 1908 N.D. 45) Di-n-Octylphthalate 35.05 149 2062 N.D. 46) Benzo(b)fluoranthene 36.13 252 1465 N.D. 47) Benzo(k)fluoranthene 36.13 252 1465 N.D. 48) Benzo(a)pyrene 37.12 252 2685 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LBA.D GCMS1126.M Tue Jan 15 11:12:55 2002 Page 2

NYC-WTC_000017885

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NYC-WTC_000017885Source: NYC Law Department, mirrored locally

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