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GCMS analysis results for sample AD30472, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30472 conducted on January 24, 2002.

NYC-WTC_000017931–000017939

Folder label: “GCMS X 12/14/01 A 12/31/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\DEC3101\30472.D Vial: 7 Acq On : 31 Dec 2001 4:48 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 11:14 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.00 178 789 N.D. 3 4) Anthracene 25.00 178 789 N.D. 35) Di-n-butylphthalate 27.03 149 6398 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.51 149 479 N.D. 41) Benzo(a)anthracene 33.02 228 5334 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 13715 N.D. 43) Chrysene 33.02 228 5334 N.D. 45) Di-n-Octylphthalate 35.07 149 1221 N.D. 46) Benzo(b)fluoranthene 36.10 252 463 N.D. 47) Benzo(k)fluoranthene 36.10 252 703 N.D. 48) Benzo(a)pyrene 37.12 252 3979 N.D. 4 9) Indeno(1,2,3 -cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30472.D GCMS1126.M Tue Jan 15 11:15:08 2002 Page 2

NYC-WTC_000017934

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NYC-WTC_000017934Source: NYC Law Department, mirrored locally

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