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GCMS analysis results for sample AD30490, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30490 conducted on January 24, 2002.

NYC-WTC_000017913–000017921

Folder label: “GCMS X 12/14/01 A 12/31/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC3101\30490.D Vial: 12 Acq On : 31 Dec 2001 9:40 pm Operator: 209 GALOS Sample : gems scan 12/14fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 11:22 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ' : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.99 178 665 N.D. 34) Anthracene 24.99 178 665 N.D. 35) Di-n-butylphthalate 27.07 149 2387 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 3945 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 5180 N.D. 43) Chrysene 33.02 228 3945 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.11 252 3095 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30490.D GCMS1126.M Tue Jan 15 11:22:54 2002 Page 2

NYC-WTC_000017916

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NYC-WTC_000017916Source: NYC Law Department, mirrored locally

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