Document showing calibration results for GCMS analysis of volatile organic compounds on December 31, 2001.
NYC-WTC_000017883–000017893Folder label: “GCMS X 12/14/01 A 12/31/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC3101\LBA.D Vial: 5 Acq On : 31 Dec 2001 2:51 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 15 11:12 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title ’ : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 650279 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 2544272 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.56 164 1301526 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 1808492m 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1107618 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 601871 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.07 235 109438 5.50 ug/mL 0.00 Spiked Amount 5.000 Recovery = 110.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.24 74 284 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 13.50 82 245 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.24 165 114 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2 -Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration LBA.D GCMS1126.M Tue Jan 15 11:12:52 2002 Page 1
NYC-WTC_000017884
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