NYC 9/11 Public Portal Document
Quantitation Reports (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2701\30426.D Vial: 23
Acq On : 28 Dec 2001 11:28 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Dec 31 12:19 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update ’: Fri Dec 14 12:19:30 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 1079887 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 4159467 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.56 164 2115045 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.98 188 3168694m 20.00 ug/1 -0.01
38) Chrysene-dl2 33.02 240 1964485 20.00 ug/1 -0.01
44) Perylene-dl2 37.12 264 1146695 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 204607 4.46 ug/mL 0.00
Spiked Amount 5.000 Recovery = 89.20%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.11 74 4450 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichiorobenzene 0.00 146 0 N.D. '
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 13.26 77 198 N.D.
12) 1sophorone 13.50 82 333 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.33 128 1357 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocycloperitadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 1 20.27 163 989 N.D.
21) 2,6-Dinitrotoluene 20.27 165 525 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 20.57 153 142 N.D.
24) 2,4-Dinitrotoluene 21.33 165 277 N.D.
25) Diethylphthalate 22.13 149 2534 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30426.D GCMS1126.M Mon Dec 31 12:19:44 2001 Page 1
NYC-WTC_000017726
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