NYC 9/11 Public Portal Document
Library Search Compound Report
Data File M:\INSTRU-1\2 0 9\DATA\JAN0 802\LBB.D Vial: 18
Acq On 9 Jan 2002 5:55 am Operator: 209 GALOS
Sample gems scan 12/20a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 7 Benzoic acid, 2,5-bis(trimethy Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
22.64 0.50 ug/1 148629 Phenanthrene-dl0 24.81
Hit# Of 5 Tent, ive ID MW MolForm CAS# Qual
1 Benzoic acid 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 35
2 3-Isopropo: -1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28
3 Benzeneet namine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25
4 Trisilo: .ne. 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25
Abundance Scan 1917 (22.641 min): LBB.D (-) m/z 73.00 1 00.00%
73
5000
147 355 —
221
191. [ 251, 281 I ■ ■ i ■ ■
22.40 22.60 22.80 23.00
45
—
:7
117
■' ein rfi* Pi | । .327 j 41 . .................. m/z 147.00 28.19%
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy), trimethyls
73
355
5000 rW, । . . . . । ■ 1
22.40 22.60 22.80 23.00
45 m/z 355.05 26.79%
147 179 223 267 297 |
• • i • • • • , • ■ 1 • I ■ ■ 1111 1 1 1 I 11 ' ' I 1 1 1 1 I' 1 1
miz-> 50 100 150 200 250 300 350 400 450 500 ’ 550
Abundance #60503; 3-Isopropoxy-1.1,1.7.7.7-hexamethyl-3,5,5-tris(trim
73
T
22.40 22.60 22.80 23.00
5000 m/z 221.05 19.22%
147
221 281 327 415 519 561
Td,dn/BT11n/5n[2/2/k/n1mm/n1n/m/m/d/nn01/0/100nmn/0/n/010/no/01/8.8
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methytene] ‘ 1 1 * ‘
■' 1 1 I ' ' ' 1 I 1 1
73 355 22.40 22.60 22.80 23.00
m/z 281.10 14.95%
5000
45
208 251 281 386 458 548
1 ' i ' ’ 1l*aanno/a/a/n’/a/ana’ahaalooam*//’//a010011/a/n/na)/d* *
m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00
LBB.D GCMS0103.M Thu Jan 10 16:15:35 2002 Page 7
NYC-WTC_000017554
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