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GCMS blank analysis results for sample AD30605, Jan 2002

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Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.

NYC-WTC_000017542–000017555

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File M:\INSTRU-1\2 0 9\DATA\JAN0 802\LBB.D Vial: 18 Acq On 9 Jan 2002 5:55 am Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Benzoic acid, 2,5-bis(trimethy Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 22.64 0.50 ug/1 148629 Phenanthrene-dl0 24.81 Hit# Of 5 Tent, ive ID MW MolForm CAS# Qual 1 Benzoic acid 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 35 2 3-Isopropo: -1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 28 3 Benzeneet namine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 4 Trisilo: .ne. 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 Abundance Scan 1917 (22.641 min): LBB.D (-) m/z 73.00 1 00.00% 73

5000 147 355 — 221 191. [ 251, 281 I ■ ■ i ■ ■ 22.40 22.60 22.80 23.00 45 — :7 117 ■' ein rfi* Pi | । .327 j 41 . .................. m/z 147.00 28.19% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy), trimethyls 73 355

5000 rW, । . . . . । ■ 1 22.40 22.60 22.80 23.00 45 m/z 355.05 26.79% 147 179 223 267 297 | • • i • • • • , • ■ 1 • I ■ ■ 1111 1 1 1 I 11 ' ' I 1 1 1 1 I' 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 ’ 550 Abundance #60503; 3-Isopropoxy-1.1,1.7.7.7-hexamethyl-3,5,5-tris(trim 73 T 22.40 22.60 22.80 23.00 5000 m/z 221.05 19.22% 147

221 281 327 415 519 561 Td,dn/BT11n/5n[2/2/k/n1mm/n1n/m/m/d/nn01/0/100nmn/0/n/010/no/01/8.8 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methytene] ‘ 1 1 * ‘ ■' 1 1 I ' ' ' 1 I 1 1 73 355 22.40 22.60 22.80 23.00 m/z 281.10 14.95% 5000

45 208 251 281 386 458 548 1 ' i ' ’ 1l*aanno/a/a/n’/a/ana’ahaalooam*//’//a010011/a/n/na)/d* * m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00

LBB.D GCMS0103.M Thu Jan 10 16:15:35 2002 Page 7

NYC-WTC_000017554

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GCMS calibration results · Box DEP Box 16

NYC-WTC_000017533

Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

Filed in the same folder

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