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GCMS analysis results for sample AD30633, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.

NYC-WTC_000017210–000017232

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : M:\INSTRU~1\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.618 276 280 308 rBV 420176 1314677 13.70% 2.273% 2 11.134 658 663 673 rBV 62173 153263 1.60% 0.265% 3 11.675 717 722 752 rBV 2591604 6742572 70.28% 11.657% 4 14.310 999 1009 1016 rBV 600566 1298103 13.53% 2.244% 5 15.283 1109 1115 1144 rBV 3464470 8481285 88.40% 14.663%

6 17.450 1344 1351 1361 rBV2 1371456 2966408 30.92% 5.129% 7 18.157 1422 1428 1438 rBV 122797 256342 2.67% 0.443% 8 20.277 1653 1659 1670 rBV 1068382 2300074 23.97% 3.977% 9 20.562 1683 1690 1707 rBV 3869310 8955796 93.35% 15.484% 10 21.048 1738 1743 1764 rBV 87765 416437 4.34% 0.720%

11 22.793 1926 1933 1940 rBV 686840 1473925 15.36% 2.548% 12 24.987 2161 2172 2205 rBV3 3339842 9594219 100.00% 16.588% 13 26.887 2373 2379 2387 rBV 325204 714270 7.44% 1.235% 14 28.659 2565 2572 2579 rBV 250405 550987 5.74% 0.953% 15 30.063 2720 2725 2735 rBV 354032 776562 8.09% 1.343%

16 30.247 2739 2745 2753 rW 208419 488372 5.09% 0.844% 17 31.716 2899 2905 2916 rBV 177676 428900 4.47% 0.742% 18 33.029 3041 3048 3068 rBV2 2229170 6374460 66.44% 11.021% 19 34.378 3189 3195 3208 rBV2 98592 306031 3.19% 0.529% 20 35.572. 3318 3325 3336 rBV2 58688 195838 2.04% 0.339%

21 36.719 3443 3450 3460 rBV2 31031 114100 1.19% 0.197% 22 37.123 3486 3494 3519 rBV 1215360 3937242 41.04% 6.807%

Sum of corrected areas: 57839863

30633.D GCMS0103.M Thu Jan 10 15:23:03 2002

NYC-WTC_000017215

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NYC-WTC_000017215Source: NYC Law Department, mirrored locally

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