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GCMS analysis log for sample AD30608

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.

NYC-WTC_000017192–000017209

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017197
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NYC 9/11 Public Portal Document 5 LSC Area Percent Report ‘Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D Vial: 32 Acq On : 28 Dec 2001 8:16 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Method. : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thre: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 signal : TIC peak R.T. first max last PK peak peak peak % of # = min scan scan scan TY height area % max. total 1 7,131 222 227 234 rBV3 33936 130123, 1.51% 0.274% 2 7.618 276 280 293 rBV 367941 1116872 13.00% 2.356% 3 11.676 717 722 752 rBV 2282452 6351977 73.95% 13.397% 4 12.511 805 813 824 rVB 23266 97254 1.13% 0.205% 5 14.310 999 1009 1017 rBV 235656 518333 6.03% 1.093% 6 15.284 1109 1115 1134 rBV 3236629 7936867 92.40% 16.740% 7° +17.450 1345 1351 1362 rBV 561530 1193222 13.89% 2.517% 8 20.278 1652 1659 1667 rBV 394688 839991 9.78% 1.772% 9 20.562 1683 1690 1707 rBV 3710848 8589317 100.00% 18.116% 10 21.067 1738 1745 1765 rBV2 45767 233516 2.72% 0.493% 11 22.793 1926 1933 1941 rBV 232503 499871 5.82% 1.054% 12 24.987 2163 2172 2210 rBV2 2990330 8501933 98.98% 17.931% 13 26.888 2374 2379 2386 rBV 95299 204536 2.38% 0.431% 14 28.659 2566 2572 2579 rBV 62344 139827 1.63% 0.295% 15 30.064 2719 2725 2738 rBV 413437 887965 10.34% 1.873% 16 30.248 2738 2745 2752 rvVB 51714 124064 1.44% 0.262% 17 31.716 2900 2905 2912 rvB 38852 94416 1.10% 0.199% 18 33.020 3040 3047 3067 rBV2 2145664 5829561 67.87% 12.295% 19 35.572 3320 3325 3333 rBV 29441 93258 1.09% 0.197% 20 37,114 3485 3493 3521 rBV2 1196511 4031049 46.93% 8.502% Sum of corrected areas: 47413952 30608.D GCMS0103.M Thu Jan 10 15:07:34 2002 NYC-WTC_000017197

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NYC-WTC_000017197Source: NYC Law Department, mirrored locally

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