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GCMS analysis results for sample AD30607, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.

NYC-WTC_000017171–000017191

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File : M:\INSTRU~1\209\DATA\DEC2701\30607.D Vial: 33 Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.617 276 280 292 rBV 329306 922486 10.98% 1.931% 2 7.755 292 295 317 rVB 54214 221136 2.63% 0.463% 3 11.675 717 722 752 rBV 2251004 6215004 73.96% 13.007% 4 14.310 1003 1009 1018 rVB 223902 471111 5.61% 0.986% 5 15.283 1109 1115 1135 rBV 3099699 7732850 92.03% 16.184%

6 17.449 1345 1351 1360 rBV 730895 1524072 18.14% 3.190% 7 20.277 1653 1659 1667 rBV 577561 1205555 14.35% 2.523% 8 20.561 1683 1690 1708 rBV 3529851 8384119 99.78% 17.547% 9 21.048 1738 1743 1761 rBV2 66116 343901 4.09% 0.720% 10 22.792 1924 1933 1940 rBV 357851 758689 9.03% 1.588%

11 24.986 2163 2172 2201 rBV 2956261 8402693 100.00% 17.586% 12 26.887 2374 2379 2387 rVB 154569 327950 3.90% 0.686% 13 28.658 2563 2572 2580 rBV 104144 235258 2.80% 0.492% 14 30.063 2719 2725 2734 rBV 358033 786015 9.35% 1.645% 15 30.247 2738 2745 2752 rW 90109 204376 2.43% 0.428%

16 31.716 2899 2905 2914 rBV 64795 161434 1.92% 0.338% 17 33.019 3040 3047 3073 rBV2 2029893 5828987 69.37% 12.200% 18 34.378 3189 3195 3202 rBV 35450 103268 1.23% 0.216% 19 37.123 3486 3494 3518 rBV2 1169076 3951488 47.03% 8.270%

Sum of corrected areas: 47780392

30607.D GCMS0103.M Thu Jan 10 14:55:11 2002

NYC-WTC_000017176

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NYC-WTC_000017176Source: NYC Law Department, mirrored locally

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