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GCMS analysis results for sample AD30601, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.

NYC-WTC_000017126–000017138

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : M:\INSTRU~1\209\DATA\DEC2701\LBB.D Vial: 24 Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.611 276 280 312 rBV 493804 1417361 14.27% 2.728% 2 11.678 718 723 755 rBV 2944609 7513760 75.63% 14.460% 3 14.304 1004 1009 1016 rBV 95674 216772 2.18% 0.417% 4 15.277 1110 1115 1134 rBV 3794370 9317882 93.79% 17.932% 5 17.452 1344 1352 1360 rBV 314596 654866 6.59% 1.260%

6 20.280 1653 1660 1667 rBV 220711 475005 4.78% 0.914% 7 20.565 1684 1691 1715 rBV 4083177 9935077 100.00% 19.120% 8 21.088 1741 1748 1756 rBV3 39896 175682 1.77% 0.338% 9 22.786 1929 1933 1939 rBV 132922 281018 2.83% 0.541% 10 24.980 2163 2172 2204 rBV2 3464834 9708211 97.72% 18.683%

11 26.890 2375 2380 2385 rBV 49998 105025 1.06% 0.202% 12 30.066 2720 2726 2740 rBV 453677 1045629 10.52% 2.012% 13 33.022 3041 3048 3074 rBV2 2461775 6642887 66.86% 12.784% 14 37.126 3486 3495 3523 rBV 1337225 4472656 45.02% 8.608%

Sum of corrected areas: 51961831

LBB.D GCMS0103.M Thu Jan 10 13:58:12 2002

NYC-WTC_000017130

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NYC-WTC_000017130Source: NYC Law Department, mirrored locally

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