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GCMS unknowns analysis report for sample AD31340, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31340 using GCMS on February 11, 2002.

NYC-WTC_000017026–000017039

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000017036
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NYC 9/11 Public Portal Document 7 Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0902\31340.D Vial: 7 Acq On : 10 Jan 2002 9:24 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JOSS IESE IIS SIGHS SSIS T III GIO SSIS S SIO GIS IONS IGISII OI S fei Peak Number 4 Ethane, 1-ethoxy-1-methoxy- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.29 0.46 ug/l 76685 1,4-Dichlorobenzene-d4 11.52 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Ethane, 1-gthoxy-1-methoxy- 104 C5H1202 010471-14-4 45 2 2-PropanoY, 1-(2-methoxy-1-methylet 148 C7H1603 020324-32-7 42 3 2-Propandl, 1,1'-oxybis- 134 C6H1403 000110-98-5 40 4.2-Propanol, 1,1'-[(1-methyl-1,2-eth 192 C9H2004____——(001638-16-0 38 Abundance aes ‘Scan 664 (17.204 min): 31340. ©) | m/z 59.05 100.008 . | ‘5000 | 3 103 | 11,00. 11.20_ 11.40 11.60 ull, St i, sagptegeee PE 44.9 56.88 mz—> 20 30 40 50 60 70 80 © 100 110 120 130 | Abundance #1926: Ethane, 7-ethoxy-1-methoxy- 7 ere | te [Hes as as S| a | | [m/z 73.00 9. 90% i : 403. | mz 20.30 40 90 60.70. 80 90100. 110 120430 59 | 14.00 11.20. 11.40 11.60 ‘8000. i ns 403 m/z 103.6, 29.38 3 i it : 430 | . miz>__20 30 40 80 60 70 80 9 100 110 120 130 _ a" if Abundance #6087: 2-Propanol, 1,1’-oxybis- Do ' “1100 11.20 1140.11.60 m/z 41,0, 26.27 5000 i oY | 7 103 j | ; pn ® | | mz 20_ 39 40__80_ 60 7080. 90.100 140_ 120.130 | 14.00 14.20 11.40 11:60 | 31340.D GCMS0103.M Tue Feb 05 16:53:49 2002 Page 4 NYC-WTC_000017036

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NYC-WTC_000017036Source: NYC Law Department, mirrored locally

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