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GCMS analysis results for sample AD31345, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AD31345 conducted on February 11, 2002.

NYC-WTC_000016970–000016980

Folder label: “GCMS X 12/24/01 A 1/10/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File : C:\HPCHEM\l\DATA\JAN0902\31345.D Vial: 11 Acq On : 11 Jan 2002 1:19 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.466 261 264 277 rBV 192154 591321 11.36% 2.352% 2 7.603 277 279 298 rVB 33269 132176 2.54% 0.526% 3 11.523 702 706 727 rBV 1389605 3876727 74.47% 15.420% 4 15.122 1093 1098 1117 rBV 2381270 4929001 94.68% 19.605% 5 20.391 1666 1672 1695 rBV 2515046 5205742 100.00% 20.706%

6 24.807 2147 2153 2165 rBV2 2194922 4791575 92.04% 19.059% 7 24.954 2165 2169 2179 rVB2 16663 56825 1.09% 0.226% 8 29.884 2701 2706 2715 rBV 253247 488381 9.38% 1.943% 9 32.831 3021 3027 3044 rBV2 1320100 3036640 58.33% 12.078% 10 36.898 3463 3470 3494 rBV 706978 2032765 39.05% 8.085%'

Sum of corrected areas: 25141153

31345.D GCMS0103.M Tue Feb 05 16:57:15 2002

NYC-WTC_000016975

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NYC-WTC_000016975Source: NYC Law Department, mirrored locally

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