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GCMS analysis results for sample AD31277, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AD31277 conducted on February 11, 2002.

NYC-WTC_000016951–000016960

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000016956
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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\JAN0902\31277.D Vial: 13 Acq On : 11 Jan 2002 3:17 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.470 260 264 296 rVB 276684 894089 16.04% 3.286% 2 11.528 701 706 725 rBV 1557750 4144924 74.37% 15.233% 3 15.117 1092 1097 1112 rBV 2422052 5295637 95.01% 19.462% 4 20.387 1665 1671 1687 rBV 2699087 5573549 100.00% 20.484% 5 24.803 2146 2152 2165 rBV2 2424765 5197667 93.26% 19.102%

6 24.950 2165 2168 2181 rVB 19229 66118 1.19% 0.243% 7 29.879 2700 2705 2712 rBV 297427 590539 10.60% 2.170% 8 32.835 3021 3027 3045 rBV2 1404552 3279829 58.85% 12.054% 9 36.902 3463 3470 3490 rBV 771618 2167373 38.89% 7.965%

Sum of corrected areas: 27209725

31277.D GCMS0103.M Tue Feb 05 16:51:58 2002

NYC-WTC_000016956

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NYC-WTC_000016956Source: NYC Law Department, mirrored locally

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