GCMS blank analysis results, January 2002

NYC 9/11 Public Portal Document Rs Quantitation Report (QF Reviewed) . Data File : C:\HPCHEM\1\DATA\DEC1901\LBA.D Vial: 15 Acg On : 20 Dec 2001 3:07 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 a Inst : GC/MS 209 Mise g Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 12:23 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. Qlon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.68 152 804049 20.00 ug/l -0.02 10) Naphthalene-ds 15.27 136 3077969 20.00 ug/l = -0.03 17) Acenaphthene-di0 20.55 164 1542281 20.00 ug/l -0.02 29) Phenanthrene-d10 24.98 188 2227538m 20.00 ug/l -0.01 38) Chrysene-di2 33.01 240 1402688 20.00 ug/l -0.02 44) Perylene-di2 37.11 264 907829 20.00 ug/l -0.01 System Monitoring Compounds 37) 2,4-DDD 30.05 235 118975 3.69 ug/ml -0.02 Spiked Amount 5.000 Recovery = 73.80% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.11 74 1153 N.D. 3) bis(2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 O) N.D. 6) 1,2-Dichlorobenzene 0.00 146 0) N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0) N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 C) N.D. 9) Hexachloroethane 0.00 117 ° N.D. 11) Nitrobenzene 0.00 #77 0 N.D. 12) Isophorone 0.00 82 ° N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 ° N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 353 N.D. 16) Hexachlorobutadiene 0.00 225 0) N.D. 18) Hexachlorocyclopentadiene 0.00 237 0) N.D. 19) 2-Chloronaphthalene 0.00 162 0) N.D. 20) Dimethylphthalate 0.00 163 ) N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0) N.D. 23) Acenaphthene 20.57 153 117 N.D. 24) 2,4-Dinitrotoluene 20.93 165 689 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0) N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration LBA.D GCMS1126.M Mon Dec 31 12:23:31 2001 Page 1 NYC-WTC_000016800