GCMS blank results for sample AD29024, Dec 18 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1001\LBC.D Vial: 25 Acq On : 11 Dec 2001 12:05 pm Operator: 209 GALOS Sample : gc/ms scan ll/30a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 15:24 2001 Quant Results File: GCMS1126.RES

‘Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.67 152 1068150 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 4128320 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.55 164 2041430 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.97 188 2960963 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1872403 20.00 ug/1 -0.03 44) Perylene-dl2 37.10 264 1322191 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 175101 4.97 ug/mL -0.02 Spiked Amount 5.000 Recovery = 99.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.17 74 1218 N.D. 3) bis(2-Chloroethyl)ether 11.15 93 287 N.D. 4) 1,3-Dichlorobenzene 11.58 146 562 N.D. 5) 1,4-Dichlorobenzene 11.72 146 653 N.D. 6) 1,2-Dichlorobenzene 12.24 146 513 N.D. 7) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.54 77 205 N.D. 12) Isophorone 14.07 82 216 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 15.17 180 110 N.D. 15) Naphthalene 15.33 128 2548 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 20.65 153 466 N.D. 24) 2,4-Dinitrotoluene 21.45 165 108 N.D. 25) Diethylphthalate 22.08 149 1988 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration LBC.D GCMS1126.M Wed Dec 12 15:26:09 2001 Page 1

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