NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GCMS blank analysis results Jan 2002
Machine-extracted title · confidence 90%Blank sample analysis report for GCMS testing showing non-detect levels for target analytes.
NYC-WTC_000036350–000036359Folder label: “GCMS X 12/5/01 A 12/12/01”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC1201\LBE.D Vial: 15 Acq On : 12 Dec 2001 4:39 pm Operator: 209 GALOS Sample : gc/ms scan 12/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 10:36 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 935684 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3580372 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1778071 20.00 ug/1 -0.03 29) Phenanthrene-dlO 24.97 188 2521450 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1525927 20.00 ug/1 -0.03 44) Perylene-dl2 37.10 264 1018324 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 131474 4.38 ug/mL -0.02. Spiked Amount 5.000 Recovery = 87.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 12.98 77 282 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane. 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1674 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.01 165 690 N.D. 25) Diethylphthalate 22.11 149 486 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration LBE.D GCMS1126.M Fri Dec 21 12:37:05 2001 Page 1
NYC-WTC_000036351
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