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GCMS analysis report for sample AD30257, January 2002

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Laboratory GCMS analysis report for sample AD30257 conducted on January 9, 2002, by analyst DLV.

NYC-WTC_000016764–000016772

Folder label: “GCMS X 12/12/01 A 12/19/01

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NYC 9/11 Public Portal Document . Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\DEC3101\30257.D Vial: 57 Acq on : 2 Jan 2002 9:12 pm Operator: 209 GALOS Sample : gems scan 12/12 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS GIES SEIS SSIS CI SIE II EIS EIFS ISSO CIS DISCS EIOIIS IHS Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD RTs 7.61 3.86 ug/l 884805 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm cASs# Qual 1 3-Pentanol /3-methyl- 102 C6H140 000077-74-7 33 2 1-Butanamjne, 3-methyl- 87 C5H13N 000107-85-7 9 3 1,3-Dioxélane, 2-methyl- 88 C4H802 000497-26-7 9 4 Silane/ tetramethyl- __ 88 C4H12Si 000075-76-3 9 ‘Rburdance ==" Sean 260 (7.619 min}: 30257. () m/z ‘I 100.00 43 55 a7 7.20 7.40 7.60 7.80 _ 8.00 : ar BSL 8,2 80, OF, 198 m/z 43.05. 32.74 miz-> 40.202 30405 7100S 110 (Abundance: #63673: 3-Pentanol, 3-methyl- | | 5 | | 5000; | . - ] . 7.20 7.40 7.60 7.80 8.00 2 9 = or m/z 45.05 12.00% mz _10 20 30 4050) 7080100110 ‘Abundance HEF {-Sutanariive, 3-methyl- 30 i 7.20 740 7.60 7.80 8.00 5000 m/z 41.05 11.73% H 45 a 55 70 87 | mz—> 10. 20 30 40 50, 60. 70 80. 90 100 __110 Abundance “#62902: 1,3-Dioxolane, 2-methy- i 7.20 7.40 7.60 7.80 8.00 | m/z 71.00 6.81% : Pa ° a7 | ma> "40290. 40-9070 10110) 720 740 7.60 7.80 8.00 | 30257.D GCMS1126.M Thu Jan 03 10:31:59 2002 Page 1 NYC-WTC_000016771

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NYC-WTC_000016771Source: NYC Law Department, mirrored locally

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