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GCMS unknowns analysis report for sample AD30424, Jan 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD30424 using GCMS on January 18, 2002.

NYC-WTC_000017079–000017087

Folder label: “GCMS X 12/14/01 A 1/1/02

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NYC 9/11 Public Portal Document : Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\DEC3101\30424.D Vial: 23 Acq On : 1 Jan 2002 8:19 am Operator: 209 GALOS Sample : gems scan 12/14a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P ’ Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS IS IIIS ISSO ISS ISSO OIOEEISG TIO SISSIES ISHS Ie Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1 R.T. . EstCone Area Relative to ISTD Rory 7.61 4.46 ug/1 917070 1, 4-Dichlorobenzene-d4 11.68 Hit# of 5 Tghtative ID MW MolForm CAS# Qual 1 3-Pentanoj/ 3-methyl- 102 C6H140 000077-74-7 28 2 Silane, Hetramethyl- 88 C4H128i 000075-76-3 9 3 Butang/ 2-methoxy-2-methyl- 102 Cé6H140 000994-05-8 9 4 1,3ioxolane, 2-methyl- _ 88 C4H802 ___000497-26-7 7 ‘Roundance ‘Sean 280 (7.612 min} 50424. CF m/z 73.00 rey 43 | | 720" "740" "7.60" 7.80 8.00 50.5567, 87 103 + é c z [ee ee: A A ee he Z| del ‘Abundance #63573: 3-Pentanol, 3-methyl- | 7207.40 7.60 7.80 _8.00_ | Pa - 45 ° a m/z 44.95 11.87 mz 1020 304050) 7060 10010 ‘Abundance Wz, Slane, Biametiy | 720 740 "7.60 7.80 600 + 5000: m/z 41.0 11.54 48 i . 15 53 59 ! 88. | DE peepee pe me> "toy 8 to | | Abundance | #1761: Butane, 2-methoxy-2-methyi- 7.20 740 7.60 7.80 8.00 m/z 71.00 6.95: 5000. 55 87 aT 33 * | mace___40 20 30 40 80 60.70 80 90 100 110| 7.20 740 7.60 7.80 800 30424.D GCMS1126.M Tue Jan 15 14:50:16 2002 Page 1 NYC-WTC_000017086

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NYC-WTC_000017086Source: NYC Law Department, mirrored locally

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