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GCMS unknown compounds report, sample AD31464, Feb 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP sample AD31464 identifying unknown compounds and surrogate recovery results from February 15, 2002.

NYC-WTC_000016575–000016583

Folder label: “GCMS X 12/31/01 A 1/18/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31464.D Vial: 6 Acq On : 18 Jan 2002 8:31 pm Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.447 258 262 294 rVB 363267 1085934 16.14% 3.148% 2 11.496 698 703 726 rBV 2020604 5190637 77.13% 15.047% 3 15.094 1089 1095 1113 rBV 3124726 6531239 97.05% 18.933% 4 20.355 1662 1668 1681 rBV 3345060 6729585 100.00% 19.508% 5 24.770 2143 2149 2162 rBV2 2924006 6261856 93.05% 18.152%

6 29.847 2697 2702 2710 rBV 440336 872016 12.96% 2.528% 7 32.803 3017 3024 3039 rBV2 1908356 4533343 67.36% 13.141% 8 36.861 3459 3466 3488 rBV2 1170303 3292446 48.92% 9.544%

Sum of corrected areas: 34497056

31464.D GCMS0103.M Wed Feb 06 15:33:02 2002

NYC-WTC_000016580

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NYC-WTC_000016580Source: NYC Law Department, mirrored locally

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