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GCMS unknown compounds report, sample AD31340, Feb 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP sample AD31340 identifying unknown compounds and surrogate recovery results from February 11, 2002.

NYC-WTC_000016524–000016532

Folder label: “GCMS X 12/31/01 A 1/18/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\JAN1602\31340.D Vial: 12 Acq On : 16 Jan 2002 10:23 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.443 257 261 275 rBV 301864 795989 12.53% 2.536% 2 11.501 698 703 721 rBV 1933829 4866812 76.58% 15.508% 3 15.090 1089 1094 1113 rBV 2973261 6129145 96.45% 19.531% 4 20.360 1661 1668 1682 rBV 2974050 6354803 100.00% 20.250% 5 24.775 2142 2149 2161 rBV2 2602936 5747847 90.45% 18.316%

6 29.852 2696 2702 2708 rBV 345332 679601 10.69% 2.166% 7 32.799 3017 3023 3044 rBV2 1708804 3899032 61.36% 12.425% 8 36.866 3459 3466 3489 rBV 1052950 2908410 45.77% 9.268%

Sum of corrected areas: 31381639

31340.D GCMS0103.M Thu Feb 07 09:10:24 2002

NYC-WTC_000016529

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NYC-WTC_000016529Source: NYC Law Department, mirrored locally

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