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← Document results/DEP Box 16/GCMS X 12/26/01 A 1/15-1/16/02
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GCMS analysis results, sample AD31379, Feb 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of environmental sample AD31379 completed on 02/07/2002, showing 2,4-DDD surrogate recovery at 115%.

NYC-WTC_000016204–000016212

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File : C:\HPCHEM\1\DATA\JAN1502\31379.D Vial: 15 Acq On : 16 Jan 2002 12:40 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.441 257 261 297 rVB 374509 1155090 18.25% 3.745% 2 11.499 698 703 723 rBV 1855813 4748087 75.02% 15.393% 3 15.098 1089 1095 1113 rBV 2775295 6058915 95.74% 19.642% 4 20.358 1661 1668 1688 rBV 3076776 6328712 100.00% 20.517% 5 24.774 2142 2149 2162 rBV2 2653629 5716974 90.33% 18.534%

6 26.802 2366 2370 2375 rBV 62507 123470 1.95% 0.400% 7 29.850 2697 2702 2711 rVB 399549 819180 12.94% 2.656% 8 32.797 3017 3023 3042 rBV2 1502774 3531837 55.81% 11.450% 9 36.864 3459 3466 3486 rBV2 835031 2364228 37.36% 7.664%

Sum of corrected areas: 30846493

31379.D GCMS1126.M Mon Feb 04 15:08:48 2002

NYC-WTC_000016209

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NYC-WTC_000016209Source: NYC Law Department, mirrored locally

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