Laboratory blank analysis results, sample AE11755, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\LBA0513.D Vial: 8 • Acq On : 13 May 2002 5:46 pm Operator: Bohlk / Inst 213 Sample : LB 5/10/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Decanal (CAS) $$ n-Decanal ... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

13.55 0.07 ug/L 53607 Acenaphthene-diO 18.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanal (CAS) $$ n-Decanal $$ De... 156 C10H20O 000112-31-2 53 2 Decanal $$ n-Decaldehyde $$ n-De... 156 C10H20O 000112-31-2 50 3 Decanal (CAS) $$ n-Decanal $$ De... 156 C10H20O 000112-31-2 42 4 Octadecanal (CAS) $$ Stearaldehy. .. 268 C18H36O 000638-66-4 42 Abundance Scan 273 (13.552 min): LBA0513.D (-) m/z 57.10 100.00% 57

82 5000 71 95 112 ..................................... ... 13.20 13.40 13.60 13.80

m/z-> 0 A‘L‘‘‘ASl‘‘A‘I‘‘I* 4. " i11 ■i”" 10 20 30 40 SO 60 70 80 90 100110 120 130 140 150 160 ■ ■ 11" i • ■" i"1 'i ■"' r " m/z 55.10 67.14%

Abundance #55837: Decanal (CAS) $$ n-Decanal $$ Decyl aldehyde $$ De... 41 57 5000 82 70 13.20 13.40 13.60 13.80 112 m/z 82.10 59.81%

Ot ।।111111’ .. ।, l’*’’ Tm-j- | 1... m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130140 150 160 Abundance #55832: Decanal $$ n-Decaldehyde $$ n-Decanal $$ n-Decyl a... 43 57 13'20 13.40 ixed 13'80 5000 29 m/z 71.10 47.57% 70 82 95 112 15। . ...................................................... 128138 155 Of TITgHp ’Ii r’’’l’t 11 M’pr j r 1’| Pi i r j rrrhp i i i ij i r i 1111 ri 1i it m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130140150 160 Abundance #55835: Decanal (CAS) $$ n-Decanal $$ Decyl aldehyde $$ De­ sk ■ । ■ 13.20 13.40 13.60 13.80 ■ । • • • • ।1

m/z 70.10 47.35%

5000 70 82

95 112

0 ............................. I i...... Il 128 138 ■mY ’ I’3 "l1 ■HI Tnu—nmpmmnp—ar ‘ I' '' ‘ I ■ ■ ‘' I' m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160 13.20 13.40 13.60 13.80

BA0513.D 050802.M Tue May 14 10:36:06 2002 Page 5

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