GCMS pesticide analysis summary, sample AE10996, May 2002

2 2 - Signal #1 : C:\MSDCHEM\1\DATA\508\020514\2PESTICV.D\ECD1A.CH Vial: 7 - O O Signal #2 : C:\MSDCHEM\1\DATA\508\020514\2PESTICV.D\ECD2B.CH 2 Acq On Sample : 14 May 2002 : pest icv 1:18 pm Operator: Nefliu Inst : Instrumen CD — o "0 I Mise : Multiplr: 1.00 o C O o IntFile Signal #1: EVENTS.E IntFile Signal #2: EVENTS2.E o o' o Quant Time: May 16 13:26 2002 Quant Results File: 020504P.RES U CH 00 o — O. CD Quant Method : C:\MSDCHEM\1\METHODS\020504P.M (Chemstation Integrator) 0 Title : 508 Chlorinated Pesticides O Last Update : Thu May 16 13:26:46 2002 o Q Response via : Multiple Level Calibration C

DataAcq Meth : 508P.M 3 CD

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Response "...... ................. Signal: 2PESTICV.D\ECD1A.CH 3e+08 o o 2.5e+08

2e+08 O. C.

1.5e+08 cd o 3 1e+08 o § S C) . 8 — C9 o 5e+07 — ——

—------------------------ 1-- I--- —- 1 ri A 0 8 x i ____ __________________________ 8$ 1__ ।__ j__ —__ — _ a_ If t , 11 1 5 i ■ ■ Time 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 (Response Signal: 2PESTICV.D\ECD2B.CH t 3e+08 85

2.50+08

2e+08 R o CM

1.5e+08 5 8 1e+08 82 8ri 3 7 co 5e+07 to F — 0 ------ :1" 3 8 - §3 E---------8------------ A & $ °, $......I 1____ I________ Time 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00... 15.00 __ 16.00 17.00.... 18.00 2PESTICV.D 020504P.M Thu May 16 13:27:18 2002 .............. Page 2