NYC Law Department release
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← Document results/DEP Box 15/508 X 5/10/02 5/14/02
Document / 7 pages

GCMS pesticide analysis summary, sample AE10996, May 2002

Machine-extracted title · confidence 95%

Summary of gas chromatography-mass spectrometry results for multiple pesticides showing average concentrations and percent relative standard deviation.

NYC-WTC_000015863–000015869

Folder label: “508 X 5/10/02 5/14/02

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Scanned page image, NYC-WTC_000015868
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\020514\2PESTICV.D\ECDlA.CH Vial: 7 Signal #2 : C:\MSDCHEM\1\DATA\508\020514\2PESTICV.D\ECD2B.CH Acq On : 14 May 2002 1:18 pm Operator: Nefliu Sample : pest icv Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: EVENTS2.E Quant Time: May 16 13:26:59 2002 Quant Results File: 020504P.RES

Quant Method : C:\MSDCHEM\1\METHODS\020504P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Thu May 16 13:26:46 2002 Response via : Initial Calibration DataAcq Meth : 508P.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 13.20f 13.39f 1514.1E6 1671.7E6 0.305 0.314 Spiked Amount 0.200 Recovery 152.50% 157.00% 8 Target Compounds 1) Propachlor 8.29 7.77 207.4E6 217.4E6 0.34942 0.337 2) g-BHC 8.99 9.29 3218.6E6 3125.9E6 0.270 90 0.268 3) Heptachlor 10.04 10.23 1831.6E6 1736.OE6 0.191 06 0.187 4) Aldrin 10.68 10.91 988.2E6 1031.1E6 0.085 Ar 0.086 5) Heptachlor Epoxi 11.97 12.12 2763.5E6 2765.7E6 0.275 9 2 0.274 6) 4,4-DDE 12.70 13.16 6925.1E6 6845.3E6 0.758 9. 0.748 7) Dieldrin 13.20 13.39 1514.1E6 1671.7E6 0.140 S 0.146 8) Endrin 13.62 13.93 1306.3E6 1391.OE6 0.186 93 0.195 9) Methoxychlor 15.14 15.87 833.2E6 797.2E6 0.325 J/ 0.329

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTICV.D ।020504P.M Thu May 16 13:27:16 2002 Page 1

NYC-WTC_000015868

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NYC-WTC_000015868Source: NYC Law Department, mirrored locally

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