GCMS sample AE12764 results, June 10 2002

NYC 9/11 Public Portal Document LLbLaLy bearcr compound ueporc

Data File C:\MSDCHEM\l\DATA\060702\12764.D Vial: 4 Acq On 7 Jun 2002 11:02 am Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e • Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 17 Ethanol, 2,2,2-trichloro- Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 5.93 0.39 ug/L 232376 1,4-dichlorob'enzene-d4 9.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 / 2 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 9 3 lH-Azonine, octahydro- 127 C8H17N 005661-71-2/7 4 IH-Azonine, octahydro- 127 C8H17N 005661-71-2 5 Abundance Scan 485 (5.929 min): 12764.D (-480) (-) m/ z 43.10 100.00% 43

5000

Pmm 5.60 5.80 6.00 6.20 36 , ............................................................................................ 01 TIWTTETTTHT m/z 49.10 12.71% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #108333: Ethanol, 2,2,2-trichloro- 31

5000 ■ ■ i 1 ■ • ■ i ' ■ ■ ■ i 1 1 1 1 I 1 1 1 1 1 5.60 5.80 6.00 6.20 49 m/z 82.00 8.87%

J... 77 113 18 42 | . 61 70 84 95 1121128135 148 01 ■ ■ l ■ l ■ — 1 ■ | ■ । l'i'| ’It । | । i'i-i | ■ । 1 । । । , i , ■ [ i . ■ i । । । , . [ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance 4)3 #3877:2-Propanone, 1,1,1 -trichloro- 4 5.60 5.80 6.00 6.20 5000 m/z 125.00 7.76%

15 27 36 76 83 97 110117 125 0+ HH -hmm J TI———mmmTmmmDu 50 63

n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #744:1H-Azonine, octahydro- । > i * * * * । 30 43 56 5.60 5.80 6.00 6.20 m/z 127.00 6.69% 70 5000 127 84 38

n/z-> 0 THHP 10 20 30 15 40 r +63,01,77,491,. PHmmPP 50 60 70 112

80 90 100 110 120 130 140 150 5.60 5.80 6.00 6.20

12764.D 060302.M Mon Jun 10 10:30:07 2002 Page 20

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